一、凍干機的價格是多少
凍干機也稱為真空冷凍干燥機,是對物料進行真空冷凍,使其干燥的機器,它的應用領域廣泛,有醫用制藥凍干機、食品凍干機、實驗室凍干機等多種。凍干機的價格受到多方面因素的影響,一般凍干機的價格主要與凍干面積有關,凍干面積越大,凍干的量也越大,價格也自然上去,另外,凍干機的功能、型號、參數配置、品牌、種類等也會影響到其價格。小型的凍干機一般在兩萬元一臺左右,批量生產用的大型凍干機,其價格從十幾萬到百萬元都有。如果您需要選購凍干機的話,可以先來了解一下凍干機十大品牌。
二、凍干機原理介紹
凍(dong)干(gan)(gan)機(ji)(ji)(ji)全稱是冷(leng)凍(dong)干(gan)(gan)燥(zao)(zao)機(ji)(ji)(ji),由制(zhi)冷(leng)系(xi)統(tong)(tong)、真空(kong)系(xi)統(tong)(tong)、加熱(re)系(xi)統(tong)(tong)、電器儀表控制(zhi)系(xi)統(tong)(tong)所組(zu)成(cheng)(cheng),主(zhu)(zhu)要(yao)部件為干(gan)(gan)燥(zao)(zao)箱、凝結器、冷(leng)凍(dong)機(ji)(ji)(ji)組(zu)、真空(kong)泵、加熱(re)/冷(leng)卻裝置等,工作(zuo)時(shi),它主(zhu)(zhu)要(yao)利用的(de)(de)(de)是升華的(de)(de)(de)原理(li),將被(bei)干(gan)(gan)燥(zao)(zao)的(de)(de)(de)物(wu)品先凍(dong)結到三相(xiang)點溫度以下(xia),然后在(zai)真空(kong)條件下(xia)使(shi)物(wu)品中(zhong)的(de)(de)(de)固態(tai)水份(fen)(冰)直接(jie)升華成(cheng)(cheng)水蒸氣(qi),從物(wu)品中(zhong)排除(chu),使(shi)物(wu)品干(gan)(gan)燥(zao)(zao)。真空(kong)凍(dong)干(gan)(gan)機(ji)(ji)(ji)的(de)(de)(de)凍(dong)干(gan)(gan)分為三個過程(cheng)(cheng):(1)預(yu)凍(dong),為接(jie)下(xia)來的(de)(de)(de)升華過程(cheng)(cheng)準(zhun)備樣品。(2)初(chu)級(ji)干(gan)(gan)燥(zao)(zao),在(zai)此過程(cheng)(cheng)中(zhong),冰升華而不融化。(3)次級(ji)干(gan)(gan)燥(zao)(zao),在(zai)此過程(cheng)(cheng)中(zhong),鍵和于固體物(wu)質的(de)(de)(de)殘留水分被(bei)除(chu)去,從而留下(xia)干(gan)(gan)燥(zao)(zao)樣品,完成(cheng)(cheng)凍(dong)干(gan)(gan)。
三、凍干機的使用方法
1、將待凍干的樣品在冰箱中凍好,同時應預先用封口膜或保鮮膜封好瓶口,并扎好小孔。2、開(kai)機(ji)前(qian)檢查(電(dian)(dian)源、真(zhen)(zhen)空(kong)(kong)(kong)泵(beng)等):(1)真(zhen)(zhen)空(kong)(kong)(kong)泵(beng)置于地面,與(yu)主機(ji)保持一定(ding)高度差。防止突發(fa)停電(dian)(dian)產生(sheng)返油。若發(fa)生(sheng)停電(dian)(dian)事故,應(ying)(ying)立(li)即擰(ning)開(kai)充(chong)(chong)氣(qi)閥充(chong)(chong)氣(qi),盡快取(qu)出樣(yang)品(pin)(pin)。(2)真(zhen)(zhen)空(kong)(kong)(kong)泵(beng)油應(ying)(ying)該定(ding)期更換,注意保養和維護。油量通過(guo)玻璃(li)窗口(kou)來觀察,最(zui)好(hao)控制在2/3左(zuo)右,過(guo)多(duo)容易出現(xian)噴油現(xian)象,過(guo)少容易出現(xian)真(zhen)(zhen)空(kong)(kong)(kong)度不足。3、打開(kai)電(dian)(dian)源總(zong)開(kai)關,按“制冷(leng)”鍵(jian),儀器使用(yong)前(qian)需(xu)要制冷(leng)半(ban)小時。4、將(jiang)待(dai)凍(dong)干(gan)的樣(yang)品(pin)(pin)從冰箱中取(qu)出放好(hao),扣上有機(ji)玻璃(li)罩(zhao),檢查“○”型圈(quan)是(shi)否密封(feng)好(hao)。然后(hou)按下充(chong)(chong)氣(qi)閥上的不銹鋼片,拔出小管(guan)將(jiang)儀器密封(feng)。5、按“真(zhen)(zhen)空(kong)(kong)(kong)計”鍵(jian),真(zhen)(zhen)空(kong)(kong)(kong)度顯示;再按“真(zhen)(zhen)空(kong)(kong)(kong)泵(beng)”鍵(jian),真(zhen)(zhen)空(kong)(kong)(kong)泵(beng)工作。6、凍(dong)干(gan)結束(shu)后(hou),首先擰(ning)開(kai)充(chong)(chong)氣(qi)閥充(chong)(chong)氣(qi),使空(kong)(kong)(kong)氣(qi)緩慢(man)進入(ru),然后(hou)再關閉(bi)真(zhen)(zhen)空(kong)(kong)(kong)泵(beng),防止真(zhen)(zhen)空(kong)(kong)(kong)泵(beng)返油。再關閉(bi)真(zhen)(zhen)空(kong)(kong)(kong)計、制冷(leng)按鈕(niu)和總(zong)電(dian)(dian)源。最(zui)后(hou)取(qu)下有機(ji)玻璃(li)罩(zhao),將(jiang)樣(yang)品(pin)(pin)取(qu)出保存。7、最(zui)后(hou)將(jiang)凍(dong)干(gan)機(ji)冷(leng)阱內的冰塊清理掉,方便下次(ci)使用(yong)。
四、凍干機凍干需要多久
冷(leng)凍(dong)干(gan)燥機的整個凍(dong)干(gan)過(guo)程(cheng)都是(shi)在(zai)低(di)溫(wen)低(di)壓(ya)環(huan)境下進行的,是(shi)一個由低(di)溫(wen)逐漸緩慢升(sheng)(sheng)溫(wen)的過(guo)程(cheng),如果升(sheng)(sheng)溫(wen)過(guo)快、溫(wen)度(du)過(guo)高,容易導致(zhi)最終凍(dong)干(gan)產品(pin)外(wai)觀崩塌、品(pin)相不佳,凍(dong)干(gan)過(guo)程(cheng)分為:預凍(dong)、升(sheng)(sheng)華(hua)干(gan)燥、解析干(gan)燥等三(san)個階段,一般正常(chang)情況下需(xu)要24小(xiao)時左右(you),具體(ti)凍(dong)干(gan)產品(pin)不同,凍(dong)干(gan)所(suo)(suo)需(xu)要的時間也有所(suo)(suo)不同,如果是(shi)結晶點低(di)的生物制品(pin),一般需(xu)要三(san)十(shi)幾個小(xiao)時。