一、凍干機的價格是多少
凍干機也稱為真空冷凍干燥機,是對物料進行真空冷凍,使其干燥的機器,它的應用領域廣泛,有醫用制藥凍干機、食品凍干機、實驗室凍干機等多種。凍干機的價格受到多方面因素的影響,一般凍干機的價格主要與凍干面積有關,凍干面積越大,凍干的量也越大,價格也自然上去,另外,凍干機的功能、型號、參數配置、品牌、種類等也會影響到其價格。小型的凍干機一般在兩萬元一臺左右,批量生產用的大型凍干機,其價格從十幾萬到百萬元都有。如果您需要選購凍干機的話,可以先來了解一下凍干機十大品牌。
二、凍干機原理介紹
凍(dong)(dong)干(gan)(gan)(gan)機(ji)(ji)全稱(cheng)是冷(leng)凍(dong)(dong)干(gan)(gan)(gan)燥(zao)機(ji)(ji),由(you)制(zhi)冷(leng)系(xi)統、真(zhen)空(kong)(kong)(kong)系(xi)統、加熱系(xi)統、電器儀表控制(zhi)系(xi)統所組成(cheng),主要(yao)部(bu)件為(wei)干(gan)(gan)(gan)燥(zao)箱(xiang)、凝(ning)結(jie)器、冷(leng)凍(dong)(dong)機(ji)(ji)組、真(zhen)空(kong)(kong)(kong)泵、加熱/冷(leng)卻(que)裝(zhuang)置等,工作時,它主要(yao)利(li)用(yong)的(de)是升(sheng)華(hua)的(de)原理,將被干(gan)(gan)(gan)燥(zao)的(de)物(wu)品(pin)先(xian)凍(dong)(dong)結(jie)到三(san)相(xiang)點溫度以(yi)下(xia),然(ran)后(hou)在(zai)(zai)真(zhen)空(kong)(kong)(kong)條件下(xia)使物(wu)品(pin)中(zhong)(zhong)的(de)固態水份(冰)直(zhi)接升(sheng)華(hua)成(cheng)水蒸氣,從物(wu)品(pin)中(zhong)(zhong)排除,使物(wu)品(pin)干(gan)(gan)(gan)燥(zao)。真(zhen)空(kong)(kong)(kong)凍(dong)(dong)干(gan)(gan)(gan)機(ji)(ji)的(de)凍(dong)(dong)干(gan)(gan)(gan)分(fen)為(wei)三(san)個過程:(1)預凍(dong)(dong),為(wei)接下(xia)來的(de)升(sheng)華(hua)過程準備樣品(pin)。(2)初級干(gan)(gan)(gan)燥(zao),在(zai)(zai)此(ci)過程中(zhong)(zhong),冰升(sheng)華(hua)而(er)不融化。(3)次級干(gan)(gan)(gan)燥(zao),在(zai)(zai)此(ci)過程中(zhong)(zhong),鍵和(he)于固體(ti)物(wu)質的(de)殘(can)留(liu)(liu)水分(fen)被除去,從而(er)留(liu)(liu)下(xia)干(gan)(gan)(gan)燥(zao)樣品(pin),完成(cheng)凍(dong)(dong)干(gan)(gan)(gan)。
三、凍干機的使用方法
1、將待凍干的樣品在冰箱中凍好,同時應預先用封口膜或保鮮膜封好瓶口,并扎好小孔。2、開機前檢(jian)查(電(dian)源(yuan)、真空(kong)(kong)(kong)泵(beng)(beng)等(deng)):(1)真空(kong)(kong)(kong)泵(beng)(beng)置于地面,與主機保(bao)持一(yi)定(ding)高度差(cha)。防止突(tu)發停電(dian)產生返油(you)(you)。若(ruo)發生停電(dian)事故(gu),應立即(ji)擰(ning)開充(chong)氣(qi)(qi)(qi)(qi)閥(fa)(fa)充(chong)氣(qi)(qi)(qi)(qi),盡快取出樣(yang)品(pin)。(2)真空(kong)(kong)(kong)泵(beng)(beng)油(you)(you)應該定(ding)期更換,注意保(bao)養和維護。油(you)(you)量通過玻(bo)(bo)璃(li)(li)窗口來觀察,最好(hao)控(kong)制(zhi)在2/3左右,過多容(rong)(rong)易出現(xian)(xian)噴油(you)(you)現(xian)(xian)象,過少容(rong)(rong)易出現(xian)(xian)真空(kong)(kong)(kong)度不足。3、打開電(dian)源(yuan)總開關,按(an)“制(zhi)冷(leng)”鍵,儀器(qi)使用前需要制(zhi)冷(leng)半(ban)小時。4、將待凍干的樣(yang)品(pin)從(cong)冰(bing)箱中取出放好(hao),扣上(shang)有機玻(bo)(bo)璃(li)(li)罩(zhao),檢(jian)查“○”型圈是否密(mi)封好(hao)。然后按(an)下充(chong)氣(qi)(qi)(qi)(qi)閥(fa)(fa)上(shang)的不銹鋼片,拔出小管(guan)將儀器(qi)密(mi)封。5、按(an)“真空(kong)(kong)(kong)計(ji)”鍵,真空(kong)(kong)(kong)度顯示(shi);再(zai)(zai)按(an)“真空(kong)(kong)(kong)泵(beng)(beng)”鍵,真空(kong)(kong)(kong)泵(beng)(beng)工作。6、凍干結束后,首(shou)先擰(ning)開充(chong)氣(qi)(qi)(qi)(qi)閥(fa)(fa)充(chong)氣(qi)(qi)(qi)(qi),使空(kong)(kong)(kong)氣(qi)(qi)(qi)(qi)緩(huan)慢(man)進(jin)入,然后再(zai)(zai)關閉真空(kong)(kong)(kong)泵(beng)(beng),防止真空(kong)(kong)(kong)泵(beng)(beng)返油(you)(you)。再(zai)(zai)關閉真空(kong)(kong)(kong)計(ji)、制(zhi)冷(leng)按(an)鈕和總電(dian)源(yuan)。最后取下有機玻(bo)(bo)璃(li)(li)罩(zhao),將樣(yang)品(pin)取出保(bao)存。7、最后將凍干機冷(leng)阱內的冰(bing)塊清理掉,方便下次使用。
四、凍干機凍干需要多久
冷凍(dong)(dong)(dong)干(gan)(gan)燥機的(de)整個凍(dong)(dong)(dong)干(gan)(gan)過(guo)程(cheng)都(dou)是在低溫(wen)低壓環境下進行的(de),是一(yi)個由低溫(wen)逐(zhu)漸緩慢升溫(wen)的(de)過(guo)程(cheng),如果(guo)升溫(wen)過(guo)快、溫(wen)度(du)過(guo)高,容易導致最終凍(dong)(dong)(dong)干(gan)(gan)產品(pin)外觀崩塌、品(pin)相不(bu)(bu)佳,凍(dong)(dong)(dong)干(gan)(gan)過(guo)程(cheng)分為:預凍(dong)(dong)(dong)、升華干(gan)(gan)燥、解析干(gan)(gan)燥等三個階段,一(yi)般正常情(qing)況下需(xu)要(yao)24小時(shi)左右,具體凍(dong)(dong)(dong)干(gan)(gan)產品(pin)不(bu)(bu)同,凍(dong)(dong)(dong)干(gan)(gan)所需(xu)要(yao)的(de)時(shi)間也有所不(bu)(bu)同,如果(guo)是結晶點低的(de)生物(wu)制品(pin),一(yi)般需(xu)要(yao)三十幾個小時(shi)。